ÚvodPřístrojová technikaNMR spektrometry

NMR spektrometry



NMR SPECTROMETERS AT DEPARTMENT OF NMR

Responsible persons:   Dr. David Šaman (phone 220 183 327)
  Dr. Radek Pohl (phone 220 183 453)
  Dr. Martin Dračínský (phone 220 183 496)


Bruker Avance II™ 600 MHz equipped with Cryoprobe

Bruker Avance II 600 MHz

Magnet: Superconducting 600 MHz, UltraShield™ Plus

Console: Avance II 600, three channels, BOSS 2 (34 magnetic field homogenity corrections), BSMS 2, amplifiers BLAX2H 300/100/150 and BLAX 500

Bruker Cryoplatform, 1H and 13C channels cooled

Temperature unit B-VT 3000, BCU 05

Probeheads: triple resonance cryo-probe with ATM module (5 mm CPTCI 1H-13C/15N/D Z-GRD), inverse broad-band probe (5 mm BBI 1H/D-BB Z-GRD)


Bruker Avance I™ 500 MHz equipped with Cryoprobe

Bruker Avance I 500 MHz Cryo

Magnet: Superconducting 500 MHz, UltraShield™

Console: Avance I 500, four channels, BOSS 2 (34 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH 300/50 and 2 × BLAX 300

Bruker Cryoplatform, 1H channel cooled

Temperature unit B-VT 3000, BCU 05

Probeheads: triple resonance cryo-probe probe (5 mm TXI 1H/13C/15N Z/GRD), quadruple resonance inverse probe (5 mm QXI 1H/15N/13C/31P Z-GRD), broad-band probe with ATM module (5 mm BBO-1H Z-GRD), quadruple inverse microprobe (2.5 mm QXI 1H/15N/13C/31P Z-GRD), broad-band microprobe (2.5 mm BBO-1H Z-GRD)


Bruker Avance II™ 500 MHz with CP-MAS accessory and Oxford magnet

Bruker Avance II 500 MHz

Magnet: Superconducting 500 MHz, Oxford Instruments

Console: Avance II 500, two channels, BOSS 2 (34 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH 300/100, BLAXH 300 and BLAX 500

Temperature unit B-VT 3200, BCU 05

Solid state accessory MAS II

Probeheads: triple resonance "liquid" probe (5 mm TBO BB-1H/19F/D Z-GRD), solid-state MAS probe (3.2 mm MAS BB/1H)


Self-serviced Bruker Avance I™ 400 MHz equipped with sample changer

Bruker Avance 400 MHz

Magnet: Superconducting 400 MHz, UltraShield™

Console: Avance I 400, two channels, BOSS 2 (34 magnetic field homogenity corrections), BSMS 2, amplifier BLA2BB

Temperature unit B-VT 3200

Automatic sample changer B-ACS 120 with 120 holders

Probeheads: inverse broad-band probe with ATM module (5 mm PA BBI 1H/D-BB Z-GRD), broad-band probe (5 mm BBO-1H Z-GRD),






NMR SPECTROMETERS AT LABORATORY OF RADIOISOTOPES

Responsible person:   Dr. Tomáš Elbert (phone 220 183 456)

3H NMR BRUKER Avance II 300 MHz

3H NMR Bruker

Beside tritium probe the spectrometer is equipped with broad band probe for measuring 1H, 13C, 19F and 31P.






BENCHTOP micro-NMR SPECTROMETERS


picoSpin



picoSpin-45 NMR benchtop spectrometer

Location:   Research team of Dr. Michal Hocek
Responsible person:   Dr. Michal Hocek (phone 220 183 324)


The picoSpin-45 NMR spectrometer is a complete 45 MHz pulsed Fourier-transform liquid-phase proton NMR spectrometer in a shoebox-sized package. It includes a capillary cartridge, a permanent magnet with temperature controller and shim system, radio-frequency transmitters and receivers, digital data acquisition and signal processing, a programmable pulse sequencer, and a web-server user interface.



picoSpin-45 NMR benchtop spectrometer

Location:   Research team of Dr. Jiří Šrogl
Responsible person:   Dr. Svatava Voltrová (phone 220 183 392)