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NMR Spectrometers


GROUP OF NMR & MOLECULAR SPECTROSCOPY

Responsible persons:   Dr. David Šaman (phone 220 183 327)
  Dr. Radek Pohl (phone 220 183 453)
  Dr. Martin Draèínský (phone 220 183 496)


Bruker Avance III™ HD 600 MHz
equipped with Cryoprobe

Bruker Avance II 600 MHz

Magnet: Superconducting 600 MHz, UltraShield™ Plus

Console: Avance III HD 600, three channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH2H 300/100 and BLAX 500

Bruker Cryoplatform: 1H and 13C channels cooled

Temperature unit: BSVT, BCU 05

Probeheads: inverse triple resonance cryo-probe with ATM module (5 mm CPTCI 1H/13C/15N/D Z-GRD), inverse broad-band probe (5 mm BBI 1H/D-BB Z-GRD), micro-cryo inverse triple resonance cryo-probe with ATM module (1.7 mm CPTCI 1H/13C/15N/D Z-GRD)

Sample handling: automatic sample changer SampleCase for 24 samples

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6



Bruker Avance III™ HD 500 MHz
equipped with Cryoprobe

Bruker Avance I 500 MHz Cryo

Magnet: Superconducting 500 MHz, UltraShield™

Console: Avance III HD 500, three channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifiers BLAX2H 300/100 and BLAX 300

Bruker Cryoplatform: 1H and BB channels cooled

Temperature unit: BSVT, BCU 05

Probeheads: inverse triple resonance cryo-probe probe with ATM module (5 mm TXI 1H/13C/15N/D Z/GRD), broad-band cryo-probe probe with ATM module (5 mm CPBBO BB-1H/19F/15N/D Z/GRD), inverse quadruple resonance probe (5 mm QXI 1H/15N/13C/31P/D Z-GRD), broad-band probe with ATM module (5 mm BBO-1H/D Z-GRD), quadruple inverse microprobe (2.5 mm QXI 1H/15N/13C/31P/D Z-GRD), broad-band microprobe (2.5 mm BBO-1H/D Z-GRD)

Sample handling: automatic sample changer SampleCase for 24 samples

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6



Bruker Avance II™ 500 MHz
with CP-MAS accessory and Oxford magnet

Bruker Avance II 500 MHz

Magnet: Superconducting 500 MHz, Oxford Instruments

Console: Avance II 500, two channels, BOSS II (34 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH 300/100, BLAXH 300 and BLAX 500

Temperature unit: B-VT 3200, BCU 05

Solid state accessory: MAS II

Probeheads: triple resonance broad-band probe with ATM (5 mm PATBO BB-1H/19F/D Z-GRD), triple resonance broad-band probe (5 mm TBO BB-1H/19F/D Z-GRD), solid-state MAS probe (3.2 mm MAS BB/1H)

Workstation: Windows XP, NMR software Topspin 2.1 pl 8



Bruker Avance III™ HD 400 MHz
equipped with sample changer for 120 samples

Bruker Avance 400 MHz

Magnet: Superconducting 400 MHz, UltraShield™

Console: Avance III 400, two channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifier BLA2B

Temperature unit: BSVT, BCU 05

Probeheads: inverse broad-band probe with ATM module (5 mm PA BBI 1H/D-BB Z-GRD), broad-band probe (5 mm BBO-1H Z-GRD)

Sample handling: Automatic sample changer B-ACS 120 with 120 holders

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6



Bruker Avance III™ HD 400 MHz
equipped with Prodigy cryo-probe and sample changer for 60 samples

Bruker Avance 400 MHz

Magnet: Superconducting 400 MHz, ASCEND III™

Console: Avance III 400, two channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifier BLA2B

Temperature unit: BSVT, BCU 05

Probeheads: broad-band PRODIGY cryo-probe probe with ATM module (5 mm CPBBO BB-1H/19F/D Z-GRD)

Sample handling: automatic sample changer SampleXpress for 60 samples

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6






LABORATORY OF RADIOISOTOPES

Responsible person:   Dr. Tomáš Elbert (phone 220 183 456)

3H NMR BRUKER Avance II 300 MHz

3H NMR Bruker

Beside tritium probe the spectrometer is equipped with broad band probe for measuring 1H, 13C, 19F and 31P.






BENCHTOP micro-NMR SPECTROMETERS


picoSpin



picoSpin-45 NMR benchtop spectrometer

Location:   Research team of Dr. Michal Hocek
Responsible person:   Dr. Michal Hocek (phone 220 183 324)


The picoSpin-45 NMR spectrometer is a complete 45 MHz pulsed Fourier-transform liquid-phase proton NMR spectrometer in a shoebox-sized package. It includes a capillary cartridge, a permanent magnet with temperature controller and shim system, radio-frequency transmitters and receivers, digital data acquisition and signal processing, a programmable pulse sequencer, and a web-server user interface.



picoSpin-45 NMR benchtop spectrometer

Location:   Research team of Dr. Jiøí Šrogl
Responsible person:   Dr. Svatava Voltrová (phone 220 183 392)