GROUP OF NMR & MOLECULAR SPECTROSCOPY

Bruker Avance III™ HD 850 MHz
equipped with Cryoprobe

Magnet: Superconducting 850 MHz, Ascend™

Console: Avance III HD 850, three channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH2H 300/100 and BLAX 500

Bruker Cryoplatform: ¹H and ¹³C channels cooled

Temperature unit: BSVT, BCU 05

Probeheads: inverse triple resonance cryo-probe with ATM module (5 mm CPTCI ¹H/¹³C/¹⁵N/D Z-GRD)

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6

Bruker Avance III™ HD 600 MHz
equipped with Cryoprobe

Magnet: Superconducting 600 MHz, UltraShield™ Plus

Console: Avance III HD 600, three channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH2H 300/100 and BLAX 500

Bruker Cryoplatform: ¹H and ¹³C channels cooled

Temperature unit: BSVT, BCU 05

Probeheads: inverse triple resonance cryo-probe with ATM module (5 mm CPTCI ¹H/¹³C/¹⁵N/D Z-GRD), inverse broad-band probe (5 mm BBI ¹H/D-BB Z-GRD), micro-cryo inverse triple resonance cryo-probe with ATM module (1.7 mm CPTCI ¹H/¹³C/¹⁵N/D Z-GRD)

Sample handling: automatic sample changer SampleCase for 24 samples

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6

Bruker Avance III™ HD 500 MHz
equipped with Cryoprobe

Magnet: Superconducting 500 MHz, UltraShield™

Console: Avance III HD 500, three channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifiers BLAX2H 300/100 and BLAX 300

Bruker Cryoplatform: ¹H and BB channels cooled

Temperature unit: BSVT, BCU 05

Probeheads: inverse triple resonance cryo-probe probe with ATM module (5 mm TXI ¹H/¹³C/¹⁵N/D Z/GRD), broad-band cryo-probe probe with ATM module (5 mm CPBBO BB-¹H/¹⁹F/¹⁵N/D Z/GRD), inverse quadruple resonance probe (5 mm QXI ¹H/¹⁵N/¹³C/³¹P/D Z-GRD), broad-band probe with ATM module (5 mm BBO-¹H/D Z-GRD), quadruple inverse microprobe (2.5 mm QXI ¹H/¹⁵N/¹³C/³¹P/D Z-GRD), broad-band microprobe (2.5 mm BBO-¹H/D Z-GRD)

Sample handling: automatic sample changer SampleCase for 24 samples

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6

Bruker Avance II™ 500 MHz
with CP-MAS accessory and Oxford magnet

Magnet: Superconducting 500 MHz, Oxford Instruments

Console: Avance II 500, two channels, BOSS II (34 magnetic field homogenity corrections), BSMS 2, amplifiers BLAXH 300/100, BLAXH 300 and BLAX 500

Temperature unit: B-VT 3200, BCU 05

Solid state accessory: MAS II

Probeheads: triple resonance broad-band probe with ATM (5 mm PATBO BB-¹H/₁₉F/D Z-GRD), triple resonance broad-band probe (5 mm TBO BB-¹H/¹⁹F/D Z-GRD), solid-state MAS probe (3.2 mm MAS BB/¹H)

Workstation: Windows XP, NMR software Topspin 2.1 pl 8

Bruker Avance III™ HD 400 MHz
equipped with sample changer for 120 samples

Magnet: Superconducting 400 MHz, UltraShield™

Console: Avance III 400, two channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifier BLA2B

Temperature unit: BSVT, BCU 05

Probeheads: inverse broad-band probe with ATM module (5 mm PA BBI ¹H/D-BB Z-GRD), broad-band probe (5 mm BBO-¹H Z-GRD)

Sample handling: Automatic sample changer B-ACS 120 with 120 holders

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6

Bruker Avance III™ HD 400 MHz
equipped with Prodigy cryo-probe and sample changer for 60 samples

Magnet: Superconducting 400 MHz, ASCEND III™

Console: Avance III 400, two channels, BOSS III (36 magnetic field homogenity corrections), BSMS 2, amplifier BLA2B

Temperature unit: BSVT, BCU 05

Probeheads: broad-band PRODIGY cryo-probe probe with ATM module (5 mm CPBBO BB-¹H/¹⁹F/D Z-GRD)

Sample handling: automatic sample changer SampleXpress for 60 samples

Workstation: Linux CentOS release 5.11, NMR software Topspin 3.2 pl 6

LABORATORY OF RADIOISOTOPES

³H NMR BRUKER Avance II 300 MHz

Beside tritium probe the spectrometer is equipped with broad band probe for measuring ¹H, ¹³C, ¹⁹F and ³¹P.

BENCHTOP micro-NMR SPECTROMETERS

picoSpin-45 NMR benchtop spectrometer

The picoSpin-45 NMR spectrometer is a complete 45 MHz pulsed Fourier-transform liquid-phase proton NMR spectrometer in a shoebox-sized package. It includes a capillary cartridge, a permanent magnet with temperature controller and shim system, radio-frequency transmitters and receivers, digital data acquisition and signal processing, a programmable pulse sequencer, and a web-server user interface.

picoSpin-45 NMR benchtop spectrometer