Commercial equipment for laboratory scale extractions (Applied Separations, USA)
max. pressure: 68 MPa, max. temperature: 240°C, max. pump flow rate: 400mL/min
(the device borrowed from the IEB CAS)
Compressors and pumps
Compressor with pressure regulator (NOVA SWISS, Switzerland), max. pressure: 100 MPa
ISCO high pressure syringe pump (Teledyne Technologies, USA), max. pressure: 7500 psi
Isocratic pumps for CO2 (Ecom spol. s.r.o., Czech Republic), max. pressure: 30MPa
Isocratic pumps for liquid modifiers (Ecom spol. s.r.o., Czech Republic), max. pressure: 30MPa
Vessels
Extraction/reaction columns: 4ml -150 ml, heating jacket
Separators: 15 ml, tangential input, cooling jacket
Heating/cooling systems
Termostats and cryostats Julabo (Germany)
Thermoregulatory box: max. temperature: 60°C ; material: particleboard/plexiglass. Heated by hot air ventilator (AEG VH 227, Stiebel Eltron) connected to a control circuit equipped with a thermocouple.
Valves
Micrometer valves made in mechanical workshop of ICPF
shut off valves (Swagelok), 6-port switching valves (Ecom spol. s.r.o.)
Visualization
High pressure cell with saphire windows: 10 ml, max. pressure 6000 psi
Visualization through a movie camera
